By Baker S. G.
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Additional info for A simple meta-analytic approach for using a binary surrogate endpoint to predict the effect of inter
1). 1 1960 A New Phototropic Substance and its ESR. Taro Hayashi, Kodo Maeda, Shoji Shida and Kazuo Nakada. J. Chem. Phys. 32, 1568 (1960). Oxidn. of 1 g. lophine (2,4,5-triphenylimidazole) by 12 g. KOH in 100 cc, EtOH or by Br in EtOH gave a phototropic substance (I) considered to be an imidazole derivative. When 450 vcc. 1% K3 Fe(CN)6 aq. soln. was added during 1 hr. with stirring by an O stream to the above KOH mixt. of I, the initial violet color disappeared. Working up gave yellow prisms, m.
Of Br to the Na salt dispersed in anhyd. Et2 O yields I, which dissociates into 2 imidazolyl radicals (II). , and light favor the formation of II. Thermodynamic data of the dissocn. /◦ mole. The following I were prepd. p. given): Ph, Ph, Ph, 195◦ ; p-tolyl, Ph, Ph, 190◦ ; p-MeOC6 H4 , Ph, Ph, 146◦ ; Ph, pMeOC6 H4 , p-MeOC6 H4 , 175◦ ; p-MeOC6 H4 , p-MeOC6 H4 , p-MeOC6 H4 , 120◦ ; p-tolyl, p-tolyl, p-tolyl, ∼ 180◦ (obtained only in 95% purity); p-Me2 NC6 H4 , Ph, Ph, 103◦ (very unstable, excluded from thermodynamic studies).
The substituent effect is related to that in the intramol. charge-transfer bands of 1-(p-substituted phenyl)pyrroles. The longest wavelength absorption band of the title compd. (I) is an intramol charge-transfer band. The solvent and temp. effects are consistent with this interpretation. Studies on Nitrogen-Containing Heterocyclic Free Radicals. XXI. Dissociation Constants of Dimers of Triarylimidazolyls. P. (Mord. Gos. , Saransk, USSR). Zh. Org. Khim. ). Dissocn. of I 41 42 6. A Survey of HABI Publications (R = H, R1 = H, 3-Br, 4-Br, 3-Cl, 3-Me, 4-Me, 4-MeO; R1 = 4-Ph, R = H, 4-Br, 4-Cl, 4-MeO, 4-Me, R = 4-Ph, R1 = H, 3-Br, 4-Br, 3-Cl, 3-Me, 4-Me) was studied spectrophotometrically in one or more of C6 H6 , PhOMe, PhNO2 , and PhMe; thermodn.